SEXUAL Lubricant Database

 

Instrument Parameters

 

DART-TOFMS Instrumental Parameters

DART-TOFMS Parameter Conditions
Ionization Gas Helium
Gas Temperature 350°C
Orifice 1 Voltage 20V
Orifice 2 Voltage 5V
Ring Lens Voltage 5V
Rf Ion Guide Voltage 600V
m/z Range 60-1000 amu
Ionization Modes Positive and Negative

 

 

 

 

 

 

 

 

GC-MS Instrumental Parameters

GC Parameter Conditions
Column DB-5ms Ultra Inert
Injection Volume 1 μL
Split Ratio 100:1
Injection Temperature 250°C
Oven Initial Temperature (Hold Time) 60°C (2 min)
Oven Temperature Ramp Rate 10°C /min
Oven Temperature (Hold Time) 320°C (15 min)
Column Flow Rate 1.2 mL/min
MS Source Temperature 230°C
MS Quad Temperature 150°C
m/z Range 30-550 amu

 

 

 

 

 

 

 

 

 

 

 

 

 

ATR-FTIR Instrumental Parameters

FTIR Parameters Conditions
Beam Splitter Ge/KBr
Detector DLaTGS
Range 4000-400 cm-1
Scans 60
Resolution 4 cm-1