INSTRUMENT CONTROL PARAMETERS:    MSD-2
                            ---------------------------------------

   C:\MSDChem\1\METHODS\SP.m

Control Information
------- -----------
       Sample Inlet : GC
   Injection Source : Manual
 Injection Location : Front
             Use MS : Yes

=============================================================================
                                6890 GC METHOD
=============================================================================

OVEN
   Initial temp:  45 'C (On)               Maximum temp:  325 'C
   Initial time:  3.00 min                 Equilibration time:  0.50 min
   Ramps:
      #  Rate  Final temp  Final time
      1 15.00      150        0.00
      2 40.00      265        7.00
      3   0.0(Off)
   Post temp:  0 'C
   Post time:  0.00 min
   Run time:  19.88 min

FRONT INLET (SPLIT/SPLITLESS)           BACK INLET (SPLIT/SPLITLESS)
   Mode:  Split                            Mode:  Split
   Initial temp:  170 'C (On)              Initial temp:  250 'C (Off)
   Pressure:  8.23 psi (On)                Pressure:  0.00 psi (Off)
   Split ratio:  10:1                      Total flow:  45.0 mL/min
   Split flow:  21.3 mL/min                Gas saver:  Off
   Total flow:  26.4 mL/min                Gas type:  Helium
   Gas saver:  On
   Saver flow:  20.0 mL/min
   Saver time:  25.00 min
   Gas type:  Helium

COLUMN 1                                COLUMN 2
   Capillary Column                        Capillary Column
   Model Number:  J & W 1225532            Model Number:  Agilent 19091J-233
   DB5 MS                                  HP-5  5% Phenyl Methyl Siloxane
   Max temperature:  350 'C                Max temperature:  325 'C
   Nominal length:  30.0 m                 Nominal length:  30.0 m
   Nominal diameter:  250.00 um            Nominal diameter:  250.00 um
   Nominal film thickness:  0.25 um        Nominal film thickness:  1.00 um
   Mode:  constant flow                    Mode:  (see column 1)
   Initial flow:  1.2 mL/min               Nominal initial flow:  1.1 mL/min
   Nominal init pressure:  9.14 psi        Nominal init pressure:  9.13 psi
   Average velocity:  39 cm/sec            Average velocity:  39 cm/sec
   Inlet:  Front Inlet                     Inlet:  Front Inlet
   Outlet:  MSD                            Outlet:  MSD
   Outlet pressure:  vacuum                Outlet pressure:  vacuum

FRONT DETECTOR (NO DET)                 BACK DETECTOR (NO DET)

SIGNAL 1                                SIGNAL 2
   Data rate:  20 Hz                       Data rate:  20 Hz
   Type:  test plot                        Type:  test plot
   Save Data:  Off                         Save Data:  Off
   Zero:  0.0 (Off)                        Zero:  0.0 (Off)
   Range:  0                               Range:  0
   Fast Peaks:  Off                        Fast Peaks:  Off
   Attenuation:  0                         Attenuation:  0

COLUMN COMP 1                           COLUMN COMP 2
   (No Detectors Installed)                (No Detectors Installed)

THERMAL AUX 1                           AUX PRESSURE 3
   Use:  MSD Transfer Line Heater          Description:
   Description:                            Gas Type:  Helium
   Initial temp:  280 'C (On)              Initial pressure:  0.00 psi (Off)
   Initial time:  0.00 min
      #  Rate  Final temp  Final time
      1   0.0(Off)

AUX PRESSURE 4                          AUX PRESSURE 5
   Description:                            Description:
   Gas Type:  Helium                       Gas Type:  Helium
   Initial pressure:  0.00 psi (Off)       Initial pressure:  0.00 psi (Off)

                                        POST RUN
                                           Post Time: 0.00 min

TIME TABLE
   Time       Specifier                     Parameter & Setpoint


                               GC Injector


     Front Injector:
No parameters specified

     Back Injector:
No parameters specified

 Column 1 Inventory Number : AB006
 Column 2 Inventory Number : AB004



                        GERSTEL MPS Liquid Injection

   Syringe                 : 10ul

SAMPLE PARAMETERS
   Inj. Volume             : 1.0 uL
   Inj. Speed              : 100.00 uL/s
   Fill Volume             : 5.0 uL
   Fill Strokes            : 2

   Fill Speed              : 5.00 uL/s
   Eject Speed             : 100.00 uL/s
   Viscositiy Delay        : 2.0 s

   Air Volume              : 0.0 uL
   Pre Inj. Delay          : 0.00 s
   Post Inj. Delay         : 0.00 s
   Inj. Penetration        : 40.00 mm
   Vial Penetration        : 30.00 mm

CLEANING PARAMETERS
   Preclean Sample         : 0

   Preclean Solv.1         : 6
   Postclean Solv.1        : 6
   Fill Speed Solv.1       : 5.00 uL/s
   Viscosity Delay Solv.1  : 1.0 s
   Eject Speed Solv.1      : 50.00 uL/s

   Preclean Solv.2         : 6
   Postclean Solv.2        : 6
   Fill Speed Solv.2       : 5.00 uL/s
   Viscosity Delay Solv.2  : 1.0 s
   Eject Speed Solv.2      : 50.00 uL/s

                                MS ACQUISITION PARAMETERS


General Information
------- -----------

Tune File                : atune.u
Acquistion Mode          : Scan


MS Information
-- -----------

Solvent Delay            : 3.00 min

EM Absolute              : False
EM Offset                : 0
Resulting EM Voltage     : 1176.5

[Scan Parameters]

Low Mass                 : 41.0
High Mass                : 400.0
Threshold                : 50
Sample #                 : 3       A/D Samples    8

[MSZones]

MS Quad                  : 150 C   maximum 200 C
MS Source                : 230 C   maximum 250 C


                             END OF MS ACQUISITION PARAMETERS


                              TUNE PARAMETERS for SN:  
                        -----------------------------

 EMISSION    :      34.610
 ENERGY      :      69.922
 REPELLER    :      25.935
 IONFOCUS    :      69.278
 ENTRANCE_LE :       9.500
 EMVOLTS     :    1176.471
 AMUGAIN     :    2094.000
 AMUOFFSET   :     134.000
 FILAMENT    :       1.000
 DCPOLARITY  :       0.000
 ENTLENSOFFS :      17.318
 MASSGAIN    :      -9.000   
 MASSOFFSET  :     -10.000   


                           END OF TUNE PARAMETERS
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                              END OF INSTRUMENT CONTROL PARAMETERS
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